N-Fluoro-N'-(chloromethyl)triethylenediamine Bis(tetrafluoroborate)

Synonym : 1-(Chloromethyl)-4-fluoro-1,4-diazoniabicyclo[2.2.2]octane Bis(tetrafluoroborate)

Synonym : F-TEDA-BF4

Structure

N-Fluoro-N'-(chloromethyl)triethylenediamine Bis(tetrafluoroborate)

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General Information
TCI Product No. : F0358
Stock Status :
Unit Sizes Price Available stock
Portland, OR Tokyo *
5G 38.10 USD 4 >10
25G 137.20 USD >10 10

Status at 03:00 a.m. on Mar 19, 2010

* Items available from stock in Japan will be delivered in 10 business days

Purity / Analysis Method : >90.0%(T)
Storage :
M.F. / M.W. : C7H14B2ClF9N2=354.26
CAS Number : 140681-55-6
Related CAS Number :
MDL Number : MFCD00142607
Application

Regioselective Fluorohydroxylation Reaction of Arylallenes

Regioselective Fluorohydroxylation Reaction of Arylallenes

Regiospecific fluorination of functionalized phenols

Regiospecific fluorination of functionalized phenols

Typical procedue: To 4-(biphenyl)tributylstananne (44.3 mg) in acetone (2.0 mL) at 23ºC is added silver triflate (51.4 mg) and N-fluoro-N'-(chloromethyl)triethylenediamine bis(tetrafluoroborate) (F-TEDA-BF4) (42.5 mg). The reaction mixture is stirred for 20 min at 23ºC and then concentrated in vacuo. The residue is purified by preparative TLC eluting with hexane to give 12.0 mg of the fluorinated compound as colorless solid (70% yield).

References
Merck Index(14) : 8425
Transport Information
UNNo. : 3088
Class : 4.2
PG : II
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